ИССЛЕДОВАНИЕ ПОЛИДИСПЕРСНОСТИ МИКРО- И НАНОЧАСТИЦ В ВОДНОЙ СРЕДЕ С ИСПОЛЬЗОВАНИЕМ АНАЛИЗА ТРАЕКТОРИЙ ЧАСТИЦ
В работе сравнивались результаты, полученные методами Анализ траектории наночастиц (АТН) и динамического
рассеяния света (ДРС). Было показано, что метод АТН обладает относительно более высокой точностью и лучшей
способностью разделять смеси, содержащие одновременно частицы разных размеров в полидисперсных системах.
Результаты экспериментов показали, что метод АТН позволяет измерять полидисперсность смесей наночастиц с высокой
точностью, при этом влияние крупных агрегатов минимально.
1. M. Muzzio, J. Li, Z. Yin, I.M. Delahunty, J. Xie, and S. Sun. Monodisperse nanoparticles for catalysis and nanomedicine.
Nanoscale, 1141 (2019), 18967.
2. W.J. Stark, P.R. Stoessel, W. Wohlleben, and A.J.C.S.R. Hafner. Industrial applications of nanoparticles. Chemical Society
Reviews, 44(16) (2015), 5793-5805.
3. P.C. Lin, et al. Techniques for physicochemical characterization of nanomaterials. Biotechnology Advances, 32(4) (2014),
711-726.
4. P.H. Brown. Macromolecular size-and-shape distributions by sedimentation velocity analytical ultracentrifugation. J.
Biophys., 90 (2006), 4661.
5. W. Fraunhofer, G. Winter, C. Coester. Asymmetrical flow field-flow fractionation and multiangle light scattering for analysis
of gelatin nanoparticle drug carrier systems. Analytical Chemistry, 76 (2004), 1909-1920.
6. C.M. Maguire, M. Rösslein, P. Wick, A. Prina-Mello. Characterisation of particles in solution - a perspective on light
scattering and comparative technologies. Science and Technology of Advanced Materials, 19 (2018), 732-745.
7. Z. Jia, J. Li, L. Gao, D. Yang, and A. Kanaev. Dynamic light scattering: a powerful tool for in situ nanoparticle sizing.
Colloids and Interfaces, 7(1) (2023), 15.
8. N. Farkas, and J.A. Kramar. Dynamic light scattering distributions by any means. Journal of Nanoparticle Research, 23(5)
(2021), 120.
9. J. Caldwell, P. Taladriz-Blanco, R. Lehner, A. Lubskyy, R.D. Ortuso, B. Rothen-Rutishauser, The micro-, submicron-, and
nanoplastic hunt: A review of detection methods for plastic particles. Chemosphere, 293 (2022), 133514.
10. K. Egamberdiev, S.Z. Mirzaev, and U. Kaatze. The effect of alkali halides on the critical exponents of the 2,6-
dimethylpyridine-water system. The Journal of Physical Chemistry B, 120(48) (2016), 12379-12389.
11. Berne, B., & Pecora, R. (2000). Dynamic Light Scattering: With Applications to Chemistry, Biology, and Physics. Mineola:
Dover.
12. B. J. Frisken. Revisiting the method of cumulants for the analysis of dynamic light-scattering data. Applied Optics, 40(24)
(2001), 4087-4091.
13. Filipe, V., Hawe, A., & Jiskoot, W. (2010). Critical evaluation of nanoparticle tracking analysis (NTA) by NanoSight for the
measurement of nanoparticles and protein aggregates. Pharmaceutical Research, 27(5), 796-810.
14. J.S. Philo. A critical review of methods for size characterization of non-particulate protein aggregates. Cur. Phar. Biotech.,
10 (2009), 359-372.
15. U. Yokubov, K. Egamberdiev, B. Allaev, O. Trunilina, S. Telyaev and M. Gafurova. Silica nanoparticles hydrosol for
concrete strength increase by adding to mixing water. Journal of Chemical Technology and Metallurgy, 58 (2023), 932-936.
16. M.J. Wells, J.Y. Chen, J. Bodycomb, D. Wolgemuth, H.A. Stretz, G.A. Zacheis, and K.Y. Bell. Multi-laser nanoparticle
tracking analysis (NTA): A unique method to visualize dynamic (shear) and dynamic (Brownian motion) light scattering and
quantify nonliving natural organic matter (NNOM) in environmental water. Science of the Total Environment, 949, (2024)
174985.
17. C. Coates. New sCMOS vs. current microscopy cameras. Biophotonics International, 18(5) (2011), 24-27.
18. A.D. Kashkanova, M. Blessing, A. Gemeinhardt, D. Soulat and V. Sandoghdar. Precision size and refractive index analysis
of weakly scattering nanoparticles in polydispersions. Nature Methods, 19(5) (2022), 586-593.
19. G. Bryant, A. Alzahrani, S.J. Bryant, R. Nixon-Luke, J. Mata and R. Shah. Advanced scattering techniques for
characterisation of complex nanoparticles in solution. Advances in Colloid and Interface Science, 334 (2024), 103319.
20. K. Staroňová, J.B. Nielsen, M. Roursgaard and L.E. Knudsen. Transport of SiO₂ nanoparticles through human skin. Basic &
Clinical Pharmacology & Toxicology, 111(2) (2012), 142-144.
Copyright (c) 2026 «ВЕСТНИК НУУз»
Это произведение доступно по лицензии Creative Commons «Attribution-NonCommercial-ShareAlike» («Атрибуция — Некоммерческое использование — На тех же условиях») 4.0 Всемирная.
.jpg)
2.png)
