CONFIRMATION OF THE STRUCTURE OF AMIDE DERIVATIVES SYNTHESIZED BY THE REACTION OF PICOLIC ACID WITH TOLUIDINE ISOMERS USING MODERN METHODS OF PHYSICAL AND CHEMICAL RESEARCH

  • Dilnoza BO'RIYEVA O'zMU kimyo fakulteti tayanch doktoranti
  • Anvar ABDUSHUKUROV O'zMU kimyo fakulteti professori, k.f.d.
  • Doston NURMATOV O'zMU kimyo fakulteti tayanch doktoranti
  • Zulxumor XAJIYEVA O'zMU kimyo fakulteti bakalavri
Keywords: picolinic acid, toluidine, amide, IR spectrum, 1H NMR spectrum, 13C NMR spectrum, MASS spectrum.

Abstract

The individual properties of amides obtained from the reaction of picolinic acid with toluidine isomers and their structure were confirmed by thin-layer chromatography (TLC) and IR, NMR, MASS spectroscopy

References

A. Borowiak-Resterna et al. Photostability of hydrophobic amides of pyridine-carboxylic acid as copper extractants from chloride media // Journal of Photochemistry and Photobiology A: Chemistry, 185 (2007). -Р. 181-187.

A. Mishra et al. Synthesis, characterization and antibacterial activity of cobalt (III) complexes with pyridine-amide ligands // European Journal of Medicinal Chemistry, 43 (2008). -Р. 2189-2196.

H. Hao et al. Half-sandwich iridium (III) complexes with α-picolinic acid frameworks and antitumor applications // Journal of Inorganic Biochemistry, 192 (2019). -Р. 52-61.

E. N. Khurramov, A. K. Abdushukurov, D. M. Buriyeva, e. T. Berdimurodov* & I. Nakhatov. Synthesis of new amides based on the N-hydroxyacetylation of p-toluidine // International Journal of Mechanical and Production Engineering Research and Development (IJMPERD) ISSN (P): 2249–6890; ISSN (E): 2249–8001 Vol. 10, Issue 3, Jun 2020, -P. 6001– 6016.

Э.Н. Хуррамов, Д.М. Бўриева, А.К. Абдушукуров. Дигликол кислотанинг алмашинган ариламидларини олиш // Innovation in the modern education system: a collection scientific works of the International scientific conference. 25th December, 2020 – Washington, USA: "CESS", 2020. Part 1. –P. 193-196.

Weenawan Somphon, Kenneth, J.Haller. Crystal growth and physical characterization of picolinic acid cocrystallized with dicarboxylic acids // Journal of Crystal Growth 362 (2013). -P. 252–258.

E.M. Andrade, F.V. Molina, M.I. Florit, D. Posadas. IR response of poly(o-toluidine): spectral modifications upon redox state change // Journal of Electroanalytical Chemistry 419 (1996). -P. 15-21

R. Ramasamy. FT-IR and FT-Raman Spectral Investigation of p-toluidine // International Journal of Scientific Engineering and Applied Science Engineering and Applied Science (IJSEAS) – Vol. 2, Issue-1, January 2016 ISSN: 2395-3470 www.ijseas.com -P. 519-528

Published
2024-11-27
How to Cite
BO’RIYEVA, D., ABDUSHUKUROV, A., NURMATOV, D., & XAJIYEVA, Z. (2024). CONFIRMATION OF THE STRUCTURE OF AMIDE DERIVATIVES SYNTHESIZED BY THE REACTION OF PICOLIC ACID WITH TOLUIDINE ISOMERS USING MODERN METHODS OF PHYSICAL AND CHEMICAL RESEARCH. News of the NUUz, 3(3.1.1), 301-305. https://doi.org/10.69617/nuuz.v3i3.1.1.5406