SYNTHESIS AND RESEARCH OF THE COMPLEX COMPOUND OF 3,3'-DISULPHANIDILBIS(1H-1,2,4TRIAZOLE-5-AMINE) WITH IRON(II) SULFATE
Abstract
The article presents the method of synthesis of the complex compound of 3,3'-disulfanidylbis(1h-1,2,4-triazol-5-amine) with iron(II) sulfate. The composition and structure of the obtained complex were analyzed by physico-chemical methods of research, infrared spectroscopy, thermal analysis, X-ray structural analysis.
References
Divyang M., Ruturajsinh M., Mayank G., Dhanji P., Hitendra M. A Practical Green Visit to the Functionalized [1,2,4]Triazolo [5,1-b]quinazolin-8(4H)one Scaffolds Using the Group-Assisted Purification (GAP) Chemistry and Their Pharmacological Testing // Chemistry Select, 1031–1041 (2019). doi:10.1002/slct.201803605
Rodolfo M., Kevin A., Diana B., Alan R. Kennedyd and Mario A. Macı´ase Catalyst- and solvent-free synthesis of 2fluoro-N-(3-methylsulfanyl-1H-1,2,4-triazol-5-yl)benzamide through a microwave-assisted Fries rearrangement: X-ray structural and theoretical studies // Acta Cryst. 359–371 (2019). https://doi.org/10.1107/S2053229619002572
Rahman B., Parinaz M., Nader N., Joaquin S., Marta S. Synthesis, crystal structure and magnetic properties of a pentanuclear Mn (III) cluster with 1,2,4-triazole based Schiff base ligand // Inorganica Chimica Acta, (2020) https://doi.org/10.1016/j.ica.2020.119461
Robert Crichton Inorganic Biochemistry of Iron Metabolism// 2001 John Wiley & Sons Ltd ISBNs: 0-471-49223-X (Hardback); 0-470-84579-1 (Electronic)
Linus Pauling Institute: Micronutrient Information Centerhttps:// lpi.oregonstate.edu/mic/minerals/iron
Xayrullayev G‘.U., Kadirova Sh.A., Torambetov B.S., Botirova S.A., Mavlonova S.R. 3,3'-disulfanidilbis (1h-1,2,4-triazol5-amin) sintezi // FarDU. ILMIY XABARLAR. № 3. 2022. B.341-345.
Khayrullayev G., Torambetov B., Kadirova Sh., Vaksler Y The crystal structure of 3,3'-disulfanediyldi(1H-1,2,4-triazol-5amine) monohydrate, C4H8N8OS2 // NEW CRYSTAL STRUCTURES. -2022. doi:10.1515/ncrs-2022-0519
Saadon A., Abbas A. Synthesis and Characterization of New 1,2,4-triazole // Derivatives Form 2-Naphthol, 425-432 (2018).
Monika O., Agnieszka K., Marcin S., Highly L 4H-1,2,4-Triazole Derivatives: Synthesis, Molecular Structure and Photophysical Properties // Materials 13, 56-27 (2020). doi:10.3390/ma13245627
К.Накамото ИК спектры и спектры КР неорганических и координационных соединений // Мир. 1991. 209-388.
Dinesh R. Godhani, Anand A. Jogel, Anil M. Sanghani and Jignasu P. Mehta. Thermal study of synthesized 1,2,4-triazole compounds and their kinetic parameter evaluation // Journal of Chemical and Pharmaceutical Research 6(6):1034-1041 (2014).
Larisa C., Mihaela B., Denisa F., Daria D. Thermal study on complexes with Schiff base derived from 1,2,4-triazole as potential antimicrobial agents // Journal of Thermal Analysis and Calorimetry, 1725-1730 (2013). doi:10.1007/s10973-0122201-1
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